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Beilstein J. Org. Chem. 2016, 12, 863–873, doi:10.3762/bjoc.12.85
Graphical Abstract
Scheme 1: Synthesis of copper complexes 2–6.
Figure 1: X-ray diffraction structure of copper(II) complex 2 with thermal ellipsoids drawn at 30% probabilit...
Figure 2: ORTEP the cationic section of [Cu2(L2)2](PF6)2 (3). Thermal ellipsoids are drawn at the 30% probabi...
Figure 3: ORTEP drawing of [Cu2(L3)2](PF6)2 (4). Thermal ellipsoids are drawn at the 30% probability level. H...
Figure 4: ORTEP drawing of [Cu3(L4)3](PF6)3 (5). Thermal ellipsoids are drawn at the 30% probability level. H...
Figure 5: ORTEP drawing of [Cu3(L5)3](PF6)3 (6). Thermal ellipsoids are drawn at the 30% probability level. H...
Figure 6: Yield vs reaction time of different copper complex. The reaction was carried out in acetonitrile-d3...
Beilstein J. Org. Chem. 2015, 11, 1786–1795, doi:10.3762/bjoc.11.194
Scheme 1: Synthesis of complexes 1 and 2.
Figure 1: Structural view of 1 showing 30% thermal ellipsoids. All hydrogen atoms and PF6− were omitted for c...
Figure 2: Structural view of 2 showing 30% thermal ellipsoids. All hydrogen atoms and PF6− were omitted for c...
Scheme 2: Synthesis of 3.
Figure 3: Structural view of 3 showing 50% thermal ellipsoids. All hydrogen atoms and PF6− were omitted for c...
Scheme 3: Synthesis of complexes 4 and 5.
Figure 4: Structural view of 4 showing 30% thermal ellipsoids. All hydrogen atoms and PF6− were omitted for c...
Figure 5: Structural view of 5 showing 30% thermal ellipsoids. All hydrogen atoms and PF6− were omitted for c...